Use a Shirley background for most organic and transition metal samples to get a realistic baseline.
Fix certain parameters to maintain physical consistency (e.g., keeping a 2:3 ratio for p-orbitals). xpspeak download
Always calibrate your binding energy scale using the C 1s peak (usually at 284.8 eV) before you begin detailed fitting. Conclusion Use a Shirley background for most organic and
Adjust peak parameters like position, FWHM, and area. xpspeak download
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